• 专利标题:   Lithium iron phosphate preparation involves mixing mixed aqueous solution containing graphene oxide and copper sulfate, and then adding carbon covering and lithium iron phosphate powder to mixed aqueous solution with stirring.
  • 专利号:   CN108923045-A
  • 发明人:   GUO S, SHEN W
  • 专利权人:   UNIV SHANGHAI JIAOTONG
  • 国际专利分类:   H01M004/58, H01M004/62, H01M004/36, H01M010/0525
  • 专利详细信息:   CN108923045-A 30 Nov 2018 H01M-004/58 201911 Pages: 7 Chinese
  • 申请详细信息:   CN108923045-A CN10704060 23 Jun 2015
  • 优先权号:   CN10350757, CN10704060

▎ 摘  要

NOVELTY - Lithium iron phosphate preparation involves mixing 200 ml mixed aqueous solution containing 0.01 g graphene oxide and 0.08 g copper sulfate, and then adding 2 g carbon covering and lithium iron phosphate powder to the mixed aqueous solution with stirring at a stirring speed of 180 revolutions per minute for 2 minutes. The reacted lithium iron phosphate powder is washed with water to remove unreacted free metal ions, and then suction filtered and placed in a vacuum drying oven to give the lithium iron phosphate having a three-dimensional network structure. USE - Method for preparing lithium iron phosphate having a copper ion/graphene composite layer. ADVANTAGE - The method prepares the lithium iron phosphate in a simple, cost-effective and eco-friendly manner with higher degree of bonding and uniformity than simple mechanical mixing, and significantly improved rate discharge performance and cycle stability of lithium iron phosphate. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for a lithium iron phosphate battery, which comprises a positive electrode, a negative electrode, a separator, and an electrolyte, where the positive electrode is prepared by N-methylpyrrolidone, copper ion or graphene composite layer, a powder of lithium iron phosphate, conductive carbon black, and polyvinylidene fluoride. DESCRIPTION OF DRAWING(S) - The drawing shows a schematic scanning electron micrograph and electron spectroscopy of field emission of the product coated lithium iron phosphate powder before and after the treatment.