• 专利标题:   Preparation of graphene oxide composite adsorbent for adsorbing cation dye and contaminants, involves dripping graphene oxide solution to fly ash, adding fly ash to glutaraldehyde, crosslinking, filtering and vacuum-drying mixture.
  • 专利号:   CN104785217-A, CN104785217-B
  • 发明人:   WANG W, SHENG G, ZHU S, WANG S
  • 专利权人:   UNIV ANHUI TECHNOLOGY
  • 国际专利分类:   B01J020/24, B01J020/30
  • 专利详细信息:   CN104785217-A 22 Jul 2015 B01J-020/24 201572 Chinese
  • 申请详细信息:   CN104785217-A CN10193865 22 Apr 2015
  • 优先权号:   CN10193865

▎ 摘  要

NOVELTY - Chitosan solution with concentration of 1-5 %mass, 1 g fly ash and 1 mL chitosan solution are thoroughly mixed for 2-3 hours. The mixture is filtered and dried at 50-80 degrees C for 2-3 hours. Graphene oxide solution is dripped to 1 g fly ash and stirred. The obtained mixture is diluted with water, to form solution with solid concentration of 40 g/L. 1 g Fly ash is added to 0.5-2 mL glutaraldehyde, stirred, crosslinked at 50-80 degrees C for 2-3 hours, filtered, washed with absolute ethanol until neutral and vacuum-dried, to obtain graphene oxide composite adsorbent. USE - Preparation of graphene oxide composite adsorbent used for adsorbing cation dye and contaminants. ADVANTAGE - The method enables preparation of graphene oxide composite adsorbent having excellent graphene oxide easy-separation characteristics. DETAILED DESCRIPTION - Chitosan solution with concentration of 1-5 %mass, 1 g fly ash and 1 mL chitosan solution are thoroughly mixed for 2-3 hours. The mixture is filtered and dried at 50-80 degrees C for 2-3 hours. Graphene oxide is ultrasonically-dispersed in water, to form graphene oxide solution with concentration of 2-5 g/L. 10-20 mL Graphene oxide solution is dripped to 1 g fly ash for 8-12 hours and stirred for 2-3 hours. The obtained mixture is diluted with water, to form solution with solid concentration of 40 g/L. 1 g Fly ash is added to 0.5-2 mL glutaraldehyde, stirred, crosslinked at 50-80 degrees C for 2-3 hours, filtered, washed with absolute ethanol until neutral and vacuum-dried at 60 degrees C for 5-6 hours, to obtain graphene oxide composite adsorbent.