• 专利标题:   Preparation of graphene from agricultural and forestry waste biomass, involves adding agricultural and forestry waste biomass to water-containing reactor, hydrothermally reacting, cooling, filtering, washing, and drying.
  • 专利号:   CN106348274-A
  • 发明人:   LIU Y, SUN Z, ZHENG M, HU H, XIAO Y, LEI B, DONG H
  • 专利权人:   UNIV SOUTH CHINA AGRIC
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN106348274-A 25 Jan 2017 C01B-031/04 201730 Pages: 14 Chinese
  • 申请详细信息:   CN106348274-A CN10971603 07 Nov 2016
  • 优先权号:   CN10971603

▎ 摘  要

NOVELTY - The preparation method of graphene from agricultural and forestry waste biomass involves (i) adding agricultural and forestry waste biomass to water-containing reactor, hydrothermally reacting, cooling, filtering, washing the solid, and drying to obtain solid biological carbon, (ii) mixing base with solid biological carbon, grinding, mixing, heating and calcining in the presence of a shielding gas, stripping biological carbon from base, graphitizing, (iii) calcining the graphitized sample and immersing in an acid solution, filtering, washing, and drying to obtain few-layer graphene. USE - Preparation of graphene from agricultural and forestry waste biomass (claimed). ADVANTAGE - The environmentally-friendly method enables the preparation of graphene from agricultural and forestry waste biomass by simple process at low cost with high yield, under mild reaction conditions. DETAILED DESCRIPTION - The preparation method of graphene from agricultural and forestry waste biomass involves (i) taking agricultural and forestry waste biomass, adding to water-containing reactor, hydrothermally reacting, cooling the mixture to room temperature, filtering, washing the solid, and drying to obtain solid biological carbon, (ii) mixing base with solid biological carbon, grinding, uniformly mixing, heating and calcining in the presence of a shielding gas, stripping biological carbon from base, graphitizing, (iii) calcining the graphitized sample and immersing in an acid solution, filtering, washing the solid with water until the wash solution is neutral, and drying to obtain few-layer graphene.