• 专利标题:   Preparing fertilizer storage tank inner wall corrosion-resistant coating used for fertilizing machine, by mixing acrylic emulsion, defoamer and dispersant, adding reinforcing agent, stirring, and spraying coating on wall of tank and drying.
  • 专利号:   CN112280415-A
  • 发明人:   ZHANG J, ZHANG B, ZHU M
  • 专利权人:   LINGBI JIURUI NONGFA TECHNOLOGY CO LTD
  • 国际专利分类:   C09D133/04, C09D005/08, C09D007/61, C09D007/63
  • 专利详细信息:   CN112280415-A 29 Jan 2021 C09D-133/04 202120 Pages: 8 Chinese
  • 申请详细信息:   CN112280415-A CN11367352 30 Nov 2020
  • 优先权号:   CN11367352

▎ 摘  要

NOVELTY - Preparing fertilizer storage tank inner wall corrosion-resistant coating involves: (1) adding N-methylimidazole and maleic acid to n-bromobutane, heating, heat-preserving and stirring, washing, and vacuum drying to get a composite material, mixing with a sodium oleate solution, stirring, and performing rotary evaporation to obtain a modified reinforcing material; (2) evenly dispersing graphene and nano-bentonite in N-methylpyrrolidone to obtain a dispersion, adding the modified reinforcing material, heat-preserving and stirring, ultrasonically treating, centrifuging, leaving still, suction filtering, washing, and vacuum drying to obtain a corrosion-resistant reinforcing agent; (3) adding acrylic emulsion, defoamer and dispersant to a mixer, mixing, then adding the corrosion-resistant reinforcing agent, and continuously stirring to obtain a corrosion-resistant coating; and (4) spraying the coating on the inner wall of the fertilizer tank, then drying, and curing. USE - The method is useful for preparing fertilizer storage tank inner wall corrosion-resistant coating used for fertilizing machine. ADVANTAGE - The method improves the corrosion resistance of the coating by introducing the corrosion-resistant reinforcing agent into the coating system. DETAILED DESCRIPTION - Preparing fertilizer storage tank inner wall corrosion-resistant coating involves: (1) adding N-methylimidazole and maleic acid to n-bromobutane, heating at 72-78 degrees C, heat-preserving and stirring for 5-7 hours, washing 3 times with ethyl acetate, and vacuum drying at 55 degrees C for 5 hours to get a composite material, mixing with a sodium oleate solution, stirring for 10-12 hours, and performing rotary evaporation to dry to constant weight to obtain a modified reinforcing material; (2) evenly dispersing graphene and nano-bentonite in N-methylpyrrolidone to obtain a dispersion, adding the modified reinforcing material to the dispersion, adjusting the temperature to 50-55 degrees C, heat-preserving and stirring for 30-35 minutes, adjusting the temperature to 65-70 degrees C, ultrasonically treating for 8-10 hours, centrifuging for 40 minutes, leaving still for 2 hours, suction filtering, washing, and vacuum drying to constant weight to obtain a corrosion-resistant reinforcing agent; (3) adding acrylic emulsion, defoamer and dispersant to a mixer, mixing at 500 rpm for 30 minutes, then adding the corrosion-resistant reinforcing agent, and continuously stirring for 1 hour to obtain a corrosion-resistant coating; and (4) uniformly spraying the coating on the inner wall of the fertilizer tank, then drying and curing at a constant temperature.