• 专利标题:   Preparation of cobalt composite cobalt-nickel alloy/nitrogen-doped graphene nano-catalyst by adding citric acid, urea and graphene oxide to the medium, mixing, adding carbon cloth, reacting, and loading e.g. soluble cobalt salt.
  • 专利号:   CN114318399-A, CN114318399-B
  • 发明人:   HUANG L, LIN S, CHU W, XU B, SUN D, QU Y, REN J, YU Y
  • 专利权人:   UNIV SHAANXI SCI TECHNOLOGY
  • 国际专利分类:   B22F009/22, C25B001/04, C25B011/054, C25B011/065, C25B011/089
  • 专利详细信息:   CN114318399-A 12 Apr 2022 C25B-011/054 202243 Chinese
  • 申请详细信息:   CN114318399-A CN10010304 05 Jan 2022
  • 优先权号:   CN10010304

▎ 摘  要

NOVELTY - Preparatio of cobalt composite cobalt-nickel alloy/nitrogen-doped graphene nano-catalyst comprises adding citric acid, urea and graphene oxide to the medium, mixing to obtain suspension, adding carbon cloth, hydrothermally reacting at 160-200degrees Celsius to obtain carbon cloth precursor, loading soluble cobalt salt and soluble nickel salt, and annealing at 300-600degrees Celsius under reducing gas atmosphere. USE - The method is for preparation of cobalt composite cobalt-nickel alloy/nitrogen-doped graphene nano-catalyst ADVANTAGE - The method enables to prepare cobalt composite cobalt-nickel alloy loaded on nitrogen-doped graphene catalyst, which has low raw material price, short preparation period, simple preparation process, short safety period, and is suitable for mass production. The catalyst is directly grown on the carbon cloth to cause the lack of the adhesive, polymer as to improve the conductivity.