• 专利标题:   Preparing high voltage solid lithium iron phosphate material, comprises adding iron source, lithium source, phosphorus source, carbon source and additive into dispersant, spraying and drying, and sintering lithium iron phosphate precursor.
  • 专利号:   CN112875671-A, CN112875671-B
  • 发明人:   CHENG G, SUN J, HE Z
  • 专利权人:   HUBEI RT ADVANCED MATERIALS CO LTD
  • 国际专利分类:   C01B025/45, C01B032/00, H01M010/0525, H01M004/36, H01M004/58, H01M004/583, H01M004/62
  • 专利详细信息:   CN112875671-A 01 Jun 2021 C01B-025/45 202154 Pages: 11 Chinese
  • 申请详细信息:   CN112875671-A CN10096759 25 Jan 2021
  • 优先权号:   CN10096759

▎ 摘  要

NOVELTY - Preparing high voltage solid lithium iron phosphate material comprises (i) adding the iron source, lithium source, phosphorus source, carbon source and additive into dispersant, where molar ratio of lithium element and iron element is 1-1.1:1 and the molar ratio of iron element and phosphorus element is 0.955-0.985:1 and grinding to obtain first slurry; (ii) adding the iron source into first slurry, lithium source, phosphorus source, carbon source and additive, where the mass ratio of the iron source, lithium source, phosphorus source, carbon source and additive are added in the step (ii) and the step (i) is 0.05-2:1 and grinding to obtain second slurry; (iii) spraying and drying second slurry to obtain lithium iron phosphate precursor; and (iv) sintering lithium iron phosphate precursor under inert atmosphere and crushing. USE - The method is useful for preparing high voltage solid lithium iron phosphate material. ADVANTAGE - The material has high compaction density and charge and discharge performance. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for lithium iron phosphate material, where the compacted density of the lithium iron phosphate material is greater than or equal to 2.57 g/cm3.