• 专利标题:   Preparation of graphene-epoxy resin composite material involves mixing bisphenol A epoxy resin, epichlorohydrin and graphene, leaving mixture still, adding dicyandiamide curing agent and urea accelerator to lower layer solution and curing.
  • 专利号:   CN108530834-A
  • 发明人:   XUE Z
  • 专利权人:   ANHUI WANDONG RESIN TECHNOLOGY CO LTD
  • 国际专利分类:   C08J003/205, C08K003/04, C08L063/00
  • 专利详细信息:   CN108530834-A 14 Sep 2018 C08L-063/00 201877 Pages: 5 Chinese
  • 申请详细信息:   CN108530834-A CN10326743 12 Apr 2018
  • 优先权号:   CN10326743

▎ 摘  要

NOVELTY - Preparation of graphene-epoxy resin composite material involves mixing 20-60 parts mass bisphenol A epoxy resin, 80-100 parts mass epichlorohydrin, and 2-7 parts mass 0.5-0.7 mg/mL graphene in a reactor, stirring at 50-70 degrees C for 30-40 minutes, leaving still for 1-2 hours, removing the upper layer solution, maintaining the temperature of lower layer solution at 80-150 degrees C, stirring for 6-8 hours, adding 4-10 parts mass dicyandiamide curing agent and 0.2-1 part mass urea accelerator, mixing, ultrasonically dispersing at 65-70 degrees C for 1-2 hours, and vacuum curing at 80 degrees C for 1-2 hours, 100 degrees C for 1-2 hours, and 150 degrees C for 2-4 hours. USE - Preparation of graphene-epoxy resin composite material. ADVANTAGE - The process provides composite material which has excellent dispersibility, electroconductivity and high hardness.