• 专利标题:   Preparing graphene powder by redox method, involves heating graphene oxide solution, slowly adding hydrazine hydrate, refluxing in water bath, adding water for centrifugal separation, washing and drying to obtain reduced graphene powder.
  • 专利号:   CN110357084-A
  • 发明人:   LI A, YU M, REN W, LIU J, ZHANG F, GAO R, BAO T
  • 专利权人:   ZIBO LIANKE GRAPHENE TECHNOLOGY SERVICE CENT
  • 国际专利分类:   C01B032/192
  • 专利详细信息:   CN110357084-A 22 Oct 2019 C01B-032/192 201989 Pages: 6 Chinese
  • 申请详细信息:   CN110357084-A CN10628029 12 Jul 2019
  • 优先权号:   CN10628029

▎ 摘  要

NOVELTY - Process for preparing a graphene powder by a redox method, involves (i) heating graphene oxide solution at 60-90 degrees C, (ii) slowly adding hydrazine hydrate, refluxing at 75-85 degrees C for 12 hours in a water bath, and (iii) adding water for centrifugal separation, washing until neutral and drying to obtain a reduced graphene powder. USE - The process is useful for preparing a graphene powder by a redox method. ADVANTAGE - The method strictly controls the amount of hydrazine hydrate, reaction time and reaction temperature, prepares a high-purity reduced graphene, is simple and feasible, has fewer process flows and high yield, and is suitable for large-scale industrial production. The prepared graphene powder has excellent dispersibility, low stacking degree and does not easily agglomerate.