• 专利标题:   Composite film used for absorbing heavy metals pollutants such as lead ions, copper ions and methylene blue from industrial wastewater, comprises polyethersulfone, graphene oxide powder, porogen and dimethyl formamide.
  • 专利号:   CN104667766-A
  • 发明人:   LI J, WANG S, ZHANG D, ZHANG Q, YAN B
  • 专利权人:   UNIV FUZHOU
  • 国际专利分类:   B01D067/00, B01D069/12, B01D071/68, B01J020/26, B01J020/28, B01J020/30, C02F001/28, C02F001/44
  • 专利详细信息:   CN104667766-A 03 Jun 2015 B01D-071/68 201569 Pages: 9 Chinese
  • 申请详细信息:   CN104667766-A CN10065770 09 Feb 2015
  • 优先权号:   CN10065770

▎ 摘  要

NOVELTY - Composite film comprises 90-99 wt.% polyethersulfone, 0.01-10 wt.% graphene oxide powder, 0.5 wt.% porogen and 30 wt.% dimethyl formamide. USE - Composite film used for absorbing heavy metals pollutants such as lead ions (II), copper (II) ions and organic dyes i.e. methylene blue from industrial wastewater (claimed). ADVANTAGE - The composite film treats industrial wastewater in order to remove heavy metals pollutants in a simple and cost-effective manner. The composite film has high adsorption rate as well as capacity to achieve the purification of industrial wastewater on large scale. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for a method for preparing composite film , which involves: (A) adding graphene oxide powder to dimethyl formamide, where the mixture is subjected to sonication at 200 Watt for 2 hours; (B) cooling the agitated mixture, followed by addition of polyethersulfone; (C) degassing the formed intermediate film, which is scraped from the reaction container and then subjected into water coagulation bath comprising deionized water at 60-70 degrees C to remove the solvent; (D) adding graphene oxide and porogen to the solvent free-intermediate film, and then heating the obtained mixture at 40-60 degrees C under stirring condition for 12-24 hours to obtain casting film; and (E) rinsing the obtained casting film with deionized water, and then drying it to obtain the finished product.