• 专利标题:   Preparing mesoporous graphene useful in e.g. catalytic material comprises mixing magnesium powder and carbonate powder, pressing into block, reacting black grey powder with diluted acid and drying.
  • 专利号:   CN112794313-A, CN112794313-B
  • 发明人:   WANG C, HAN T, CUI Y, LI Q
  • 专利权人:   UNIV ZHENGZHOU
  • 国际专利分类:   C01B032/184
  • 专利详细信息:   CN112794313-A 14 May 2021 C01B-032/184 202152 Pages: 9 Chinese
  • 申请详细信息:   CN112794313-A CN10306378 23 Mar 2021
  • 优先权号:   CN10306378

▎ 摘  要

NOVELTY - Preparing mesoporous graphene comprises (a) taking magnesium powder and carbonate powder as raw material, mixing in a mol ratio of 1:4-2:1, mixing uniformly, pressing into block, placing the obtained pressing block in the liner of the sealed container, (b) placing the sealed container filled with magnesium and carbonate pressure block into a high temperature furnace, raising the temperature to 650-800 degrees C, reacting for 10-90 minutes, cooling to room temperature to obtain the black grey powder, (c) reacting the black grey powder with diluted acid, reacting for 12-36 hours, using deionized water to filter and wash to neutral, obtaining the filter cake, drying the obtained filter cake and drying to obtain the product. USE - The graphene is useful in electrochemical energy storage electrode material and catalytic material. ADVANTAGE - The method: does not have the problems of sheet stacking and agglomeration that are common in the preparation process of graphene; does not require argon protection; has high utilization rate of magnesium powder; is low cost and is easy to scale production and promotion. The graphene has rich mesopores and good electrochemical stability.