• 专利标题:   Preparing flexible self-supporting metal oxide/graphene nano-composition film, comprises e.g. dispersing graphene oxide in organic solvent into solution with metal salt, adding de-ionized water and stirring to obtain graphene oxide.
  • 专利号:   CN106876670-A
  • 发明人:   LI Y, HUANG Y, OU Z, ZHU Z, ZHANG H
  • 专利权人:   UNIV GUANGDONG TECHNOLOGY
  • 国际专利分类:   B82Y030/00, B82Y040/00, C01B032/182, C01B032/184, H01G011/36, H01M004/13, H01M004/36
  • 专利详细信息:   CN106876670-A 20 Jun 2017 H01M-004/36 201755 Pages: 12 Chinese
  • 申请详细信息:   CN106876670-A CN11236470 28 Dec 2016
  • 优先权号:   CN11236470

▎ 摘  要

NOVELTY - Preparing flexible self-supporting metal oxide/graphene nano-composition film, comprises e.g. (i) dispersing graphene oxide in organic solvent into solution with metal salt uniformly, adding de-ionized water and stirring, obtaining the dispersion of graphene oxide and metal salt; (ii) transferring the product obtained in the step (i) to the hydrothermal reaction kettle, carrying out hydro-thermal reaction at 100-140 degrees C for 0.5-12 hours, cooling naturally, obtaining hydrothermal product of metal oxide/graphene nano composition film; and (iii) carrying out vacuum filtration of the product. USE - The flexible self-supporting metal oxide/graphene nano-composition film is useful for electronic devices, lithium ion battery and electrochemical super capacitor in energy storage (claimed). DETAILED DESCRIPTION - Preparing flexible self-supporting metal oxide/graphene nano-composition film, comprises (i) dispersing graphene oxide in organic solvent into solution with metal salt uniformly, adding de-ionized water and stirring, obtaining the dispersion of graphene oxide and metal salt; (ii) transferring the product obtained in the step (i) to the hydrothermal reaction kettle, carrying out hydro-thermal reaction at 100-140 degrees C for 0.5-12 hours, cooling naturally, obtaining hydrothermal product of metal oxide/graphene nano composition film; (iii) carrying out vacuum filtration of the product obtained in the step (ii), washing, and drying to obtain metal oxide/graphene nano composition filter membrane; and (iv) dissolving metal oxide/graphene nano-composition film obtained in the step (iii) in organic solvent.