• 专利标题:   Preparing graphene glass by preparing graphene oxide using graphene oxide solution, obtaining modified glass, soaking in graphene oxide solution, reacting, soaking graphene oxide glass in solution comprising aqueous ammonia and reacting.
  • 专利号:   CN112010571-A
  • 发明人:   ZHANG L
  • 专利权人:   ZHANG L
  • 国际专利分类:   C03C017/22, C03C023/00, C09K005/14, H01B013/00, H01B005/14
  • 专利详细信息:   CN112010571-A 01 Dec 2020 C03C-023/00 202004 Pages: 8 Chinese
  • 申请详细信息:   CN112010571-A CN11018586 24 Sep 2020
  • 优先权号:   CN11018586

▎ 摘  要

NOVELTY - Method for preparing graphene glass involves (i) preparing graphene oxide by a Hummers method and configuring into a 15-25 g/l graphene oxide solution, (ii) performing surface modification of glass by performing a surface treatment with glass as a substrate, soaking in a coupling agent solution, heating at 50-70 degrees C, reacting for 1-2 hours and taking out the modified glass, (iii) preparing graphene oxide glass by soaking the modified glass in the graphene oxide solution, heating at 70-90 degrees C, reacting for 1-3 hours, taking out, washing the surface with water and drying to obtain graphene oxide glass and (iv) preparing the graphene glass by soaking the graphene oxide glass in a solution containing aqueous ammonia and hydrazine hydrate, heating at 95-100 degrees C, reacting for 1-3 hours, taking out, washing with water and drying. USE - The method is useful for preparing graphene glass used in electrically conductive and thermally conductive materials (claimed). ADVANTAGE - The method is a simple and convenient chemical method and provides the graphene glass with excellent conductivity and thermal conductivity and thickness of 1-100 atomic layers. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for the graphene glass prepared by the method, where the graphene glass is composed of the glass substrate and graphene on the glass substrate.