• 专利标题:   Preparation of graphene polyacrylate acrylonitrile friction-reducing composite coating involves cleaning substrate, drying by nitrogen blowing, adding oxidized graphite and ethanol, and performing ultrasonic dispersion.
  • 专利号:   CN104263183-A, CN104263183-B
  • 发明人:   LIU Y, LU C, MO Y, WANG L, HUANG Y
  • 专利权人:   UNIV GUANGXI
  • 国际专利分类:   C08F220/10, C08F220/44, C09D133/20, C09D007/12
  • 专利详细信息:   CN104263183-A 07 Jan 2015 C09D-133/20 201517 Pages: 5 Chinese
  • 申请详细信息:   CN104263183-A CN10522254 30 Sep 2014
  • 优先权号:   CN10522254

▎ 摘  要

NOVELTY - A graphene polyacrylate acrylonitrile friction-reducing composite coating is prepared by cleaning substrate, drying by nitrogen blowing, where if substrate is metal material, petroleum ether and n-hexane is used for cleaning and if substrate is semiconductor material, acetone and ethanol is used for cleaning, adding oxidized graphite and ethanol, performing ultrasonic dispersion to obtain 0.1-2 g/L graphene oxide dispersion, and adding surface modifying agent to modify surface of graphene oxide. USE - Preparation of graphene polyacrylate acrylonitrile friction-reducing composite coating (claimed). ADVANTAGE - Preparation process is simple and has low cost. Product has good corrosion resistance and long service life. DETAILED DESCRIPTION - A graphene polyacrylate acrylonitrile friction-reducing composite coating is prepared by cleaning substrate, drying by nitrogen blowing, where if substrate is metal material, petroleum ether and n-hexane is used for cleaning and if substrate is semiconductor material, acetone and ethanol is used for cleaning, adding oxidized graphite and ethanol, performing ultrasonic dispersion to obtain 0.1-2 g/L graphene oxide dispersion, adding surface modifying agent to modify surface of graphene oxide in which volume concentration of surface modifying agent and graphene oxide dispersion is 0.1-4 ml/L, adding hydrazine hydrate at 90 degrees C for 4 hours, centrifuging, washing, and drying to obtain graphene, dissolving acrylate in chloroform solvent to obtain 5 g/L acrylate solution, dissolving acrylonitrile in dimethylformamide to obtain 5 g/L acrylonitrile solution, mixing acrylate solution:acrylonitrile solution with ratio of 1:5-20, adding 0.1-1 g/L graphene to obtain graphene polyacrylate acrylonitrile, uniformly coating on surface of substrate, curing, placing in drying dish, and naturally cooling.