• 专利标题:   Purifying chromatographic n-heptane by adding n-heptane to UV irradiation reactor, using strong oxidizability of generated hydroxyl radical to oxidize and decompose impurities and removing impurities using chitosan-graphene oxide material.
  • 专利号:   CN110981681-A
  • 发明人:   ZHANG J, SONG J
  • 专利权人:   TIANJIN CONCORD PHARM CHEM CO LTD
  • 国际专利分类:   B01J020/24, B01J020/28, B01J020/30, C07C007/00, C07C007/12, C07C007/148, C07C009/15
  • 专利详细信息:   CN110981681-A 10 Apr 2020 C07C-007/00 202037 Pages: 6 Chinese
  • 申请详细信息:   CN110981681-A CN11037724 29 Oct 2019
  • 优先权号:   CN11037724

▎ 摘  要

NOVELTY - Method for purifying chromatographic n-heptane, involves (a) adding n-heptane to an UV irradiation reactor, irradiating under UV light at 185 nm wavelength, and using a strong oxidizability of the generated hydroxyl radical to oxidize and decompose the impurities in the n-heptane, (b) adsorbing, and removing impurities through chitosan-graphene oxide composite material, (c) dehydrating, and drying using anhydrous calcium oxide, (d) removing low-boiling impurities by distillation, (e) removing impurities by rectification, and (f) rectifying to obtain the chromatographic n-heptane. USE - The method is useful for purifying chromatographic n-heptane. ADVANTAGE - The method has excellent oxidation effect, and has fast rate and short cycle, and reduces the aggregation of graphene oxide, increases specific surface area, and improves adsorption performance, and produces 92% n-heptane with the purity of 99.4% and moisture content of below 0.01%.