• 专利标题:   Preparation of graphene solution, by forming layer of graphene on metal foil surface, scraping graphene, adding purified water to form graphene suspension, centrifuging, drying to obtain graphene particles and dissolving in water.
  • 专利号:   CN108751167-A
  • 发明人:   WU F, ZENG J, WEN J
  • 专利权人:   SHENZHEN LAIBIDE TECHNOLOGY CO LTD
  • 国际专利分类:   C01B032/184
  • 专利详细信息:   CN108751167-A 06 Nov 2018 C01B-032/184 201902 Pages: 5 Chinese
  • 申请详细信息:   CN108751167-A CN10451678 12 May 2018
  • 优先权号:   CN10451678

▎ 摘  要

NOVELTY - Preparation of graphene solution involves introducing chlorosulfonic acid solution into container, adding appropriate amount of graphite, stirring until graphite is dissolved in the chlorosulfonic acid solution, concentrating solution, pouring into reaction vessel, placing appropriate amount of metal foil in reaction vessel, introducing protective gas into reaction vessel, reacting at 900-1200 degrees C, soaking metal foil in solution until carbon inside the solution enters the metal foil, taking out metal foil, freezing in freezer compartment to form a layer of graphene on the surface, scraping graphene, pouring in container, taking upper layer of graphene suspension, introducing purified water into container to form a graphene suspension, stirring, washing liquid in the container with deionized water, ultrasonically processing to obtain homogeneous solution, centrifuging, washing, spray-drying to obtain graphene particles, dissolving graphene particles in purified water and stirring. USE - Preparation of graphene solution. ADVANTAGE - The method enables simple preparation of graphene solution with improved purity.