• 专利标题:   Preparing alpha-goethite/graphene oxide composite material by adding single-layer graphene oxide to beaker, adding water, adding ferrous sulfate powder to graphene dispersion, adding ethylene glycol, heating, washing powder, and grinding.
  • 专利号:   CN111085204-A
  • 发明人:   INVENTOR U
  • 专利权人:   HAIMEN YUANMEI ART DESIGN CO LTD
  • 国际专利分类:   B01J023/745, C02F001/30, C02F101/34, C02F101/38
  • 专利详细信息:   CN111085204-A 01 May 2020 B01J-023/745 202042 Pages: 4 Chinese
  • 申请详细信息:   CN111085204-A CN11232715 23 Oct 2018
  • 优先权号:   CN11232715

▎ 摘  要

NOVELTY - Method for preparing alpha -goethite/graphene oxide composite material, involves (a) adding 5-15 pts. wt. single-layer graphene oxide to a beaker, add 90-100 pts. wt. ultrapure water, uniformly stirring, and ultrasonically processing for 40-50 minutes, (b) adding 22-28 pts. wt. ferrous sulfate heptahydrate powder to the graphene dispersion system solution, adding 40-50 pts. wt. ethylene glycol to the beaker, stirring using a glass rod, and ultrasonically processing for 40-50 minutes, (c) adding the mixed solution to a round-bottom flask, heating in a water bath at 65-75 degrees C, refluxing for 5-7 hours to obtain a black powder, cooling, washing the powder 4-6 times with absolute ethanol, and (d) rinsing with ultrapure water for 4-6 times, leaving still for 5-6 hours, using a pipette to remove the supernatant, placing the sample in a constant temperature oven at 65-75 degrees C, drying, and grinding. USE - The method is useful for preparing alpha -goethite/graphene oxide composite material used for removing tetracycline in wastewater. ADVANTAGE - The method is simple, fast, and easy to operate. The prepared composite material has uniform morphology distribution, large specific surface area, and significant photocatalytic effect.