• 专利标题:   Preparation of graphene-polypyrrole-lithium titanate composite anode material for lithium battery, involves dissolving pyrrole monomer in solvent, adding graphene dispersion, stirring, adding lithium titanate powder, and dispersing.
  • 专利号:   CN104037395-A, CN104037395-B
  • 发明人:   YANG C, LIU D, MA Y
  • 专利权人:   HEFEI GUOXUAN HIGH TECH POWER SOURCE CO
  • 国际专利分类:   H01M004/36, H01M004/62
  • 专利详细信息:   CN104037395-A 10 Sep 2014 H01M-004/36 201480 Pages: 4 Chinese
  • 申请详细信息:   CN104037395-A CN10274231 19 Jun 2014
  • 优先权号:   CN10274231

▎ 摘  要

NOVELTY - Preparation of graphene-polypyrrole-lithium titanate composite anode material involves dissolving pyrrole monomer in a solvent, adding graphene dispersion at room temperature, stirring, adding lithium titanate powder and surfactant to resultant mixture, dispersing, maintaining obtained mixture at -2 degrees C to 5 degrees C, stirring, adding initiator, stirring, reacting, filtering, washing, and baking. The mass ratio of pyrrole monomer and initiator is 1:0.05-2. The mass ratio of pyrrole monomer and graphene is 1:0.1-1. The mass ratio of lithium titanate and graphene is 1:0.01-0.1. USE - Preparation of graphene-polypyrrole-lithium titanate composite anode material used for lithium battery. ADVANTAGE - The method enables preparation of graphene-polypyrrole-lithium titanate composite anode material with excellent electroconductivity and electrochemical property, and reduced contact resistance, with reduced energy consumption, by simple process. The graphene-polypyrrole-lithium titanate composite anode material improves performance and safety of lithium battery. DETAILED DESCRIPTION - Preparation of graphene-polypyrrole-lithium titanate composite anode material involves dissolving pyrrole monomer in a solvent, adding graphene dispersion at room temperature, stirring, adding lithium titanate powder and surfactant to resultant mixture, dispersing, maintaining obtained mixture at -2 degrees C to 5 degrees C, stirring, adding initiator, stirring, reacting, filtering, washing, and baking. The mass ratio of pyrrole monomer and initiator is 1:0.05-2. The mass ratio of pyrrole monomer and graphene is 1:0.1-1. The mass ratio of lithium titanate and graphene is 1:0.01-0.1. The mass ratio of pyrrole monomer and surfactant is 1:0.05-1.