• 专利标题:   High concentration aqueous graphene dispersion preparation by ultrasonic stripping involves adding graphite to lignin amphiphilic polymer solution and carrying out ultrasonic stripping using ultrasonic cleaning machine.
  • 专利号:   CN104876210-A, CN104876210-B
  • 发明人:   LOU H, QIU X, YANG D, ZHU D
  • 专利权人:   UNIV SOUTH CHINA TECHNOLOGY
  • 国际专利分类:   C01B031/04, C01B032/19, C01B032/194
  • 专利详细信息:   CN104876210-A 02 Sep 2015 C01B-031/04 201611 Pages: 11 Chinese
  • 申请详细信息:   CN104876210-A CN10172261 13 Apr 2015
  • 优先权号:   CN10172261

▎ 摘  要

NOVELTY - A method for preparing a water-phase graphene dispersion liquid by employing ultrasonic stripping comprises: (1) adding 1 part of graphite to 500-10000 parts of a lignin amphiphilic polymer solution with a mass concentration of 0.1-10 g/l; (2) carrying out ultrasonic stripping at 20-60 degrees C for 10-100 hours by using an ultrasonic cleaning machine; and (3) centrifugally separating to obtain to obtain a high concentration aqueous dispersion of graphene, having a concentration of 0.10 g/l. The amphiphilic polymer lignin is at least one of lignin sulfonate, lignin polyoxyethylene ethers and carboxymethylated lignin, or a lignin sulfonate and bromotetradecane copolymer. USE - Method for preparing high concentration aqueous phase graphene dispersion by ultrasonic stripping (claimed). ADVANTAGE - The method is economical and environment-friendly. The utilization rate of raw materials is improved, and the industrialization cost is reduced