• 专利标题:   Preparing graphene used in e.g. LEDs, transistors involves treating graphite with acid to form graphite oxide, mixing with metal oxide nanoparticles; and treating with acid to separate graphene.
  • 专利号:   US2012308468-A1, WO2012165753-A1, KR2012133065-A, KR1286106-B1, US9145302-B2
  • 发明人:   CHOI W K, PARK D H, KWON B W, SON D I, CHOI W
  • 专利权人:   KOREA INST SCI TECHNOLOGY
  • 国际专利分类:   B82Y030/00, C01B031/00, C01B031/04, B82B003/00, C01B031/02, C01G009/02, B82B001/00, B82Y040/00
  • 专利详细信息:   US2012308468-A1 06 Dec 2012 C01B-031/00 201282 Pages: 18 English
  • 申请详细信息:   US2012308468-A1 US193777 29 Jul 2011
  • 优先权号:   KR051557

▎ 摘  要

NOVELTY - A method (M1) for preparing graphene using metal oxide involves preparing graphite oxide by treating the surface of graphite with an acid; preparing particles where carbon is bonded to metal oxide by mixing graphite oxide with metal oxide nanoparticles; and separating graphene by treating the prepared particles with an acid. USE - For preparing graphene (claimed) e.g. used in LEDs, in transistor materials, electrode material for secondary cells, super capacitor. ADVANTAGE - The method for preparing graphene allows chemical bonding and separation through simple acid treatment process using inexpensive materials. The processing cost is low and pure graphene with few impurities can be prepared quickly in large scale. Since the particles of quasi metal oxide-graphene core-shell structure obtained as intermediate have graphene shell having very high electron mobility, they have very fast electron transfer rate. Accordingly, with fast response speed and superior optical properties, they may be used in UV sensors, LEDs, and dye-sensitized solar cells (DSSCs), replacing metal-oxide quantum dots or TiO2. DETAILED DESCRIPTION - INDEPENDENT CLAIMS are included for the following: (1) graphene prepared by the preparation method (M1); and (2) nanoparticles of metal oxide-graphene core-shell structure where graphene surrounds metal oxide nanoparticles and is prepared by reacting graphite oxide with metal oxide nanoparticles