• 专利标题:   Preparation of graphene-based and fabric-like polyaniline supercapacitor includes performing chemical reduction of expanded graphite with polyester fabric in ethanol/isopropanol, dipping, drying and heating under water bath.
  • 专利号:   CN104900422-A, CN104900422-B
  • 发明人:   PENG H, SUN H, JIE S
  • 专利权人:   UNIV FUDAN
  • 国际专利分类:   H01G011/48, H01G011/86
  • 专利详细信息:   CN104900422-A 09 Sep 2015 H01G-011/48 201602 Pages: 10 Chinese
  • 申请详细信息:   CN104900422-A CN10241685 13 May 2015
  • 优先权号:   CN10241685

▎ 摘  要

NOVELTY - Preparation of graphene-based and fabric-like polyaniline supercapacitor includes performing chemical reduction of expanded graphite with polyester fabric in 0.5-1 mg/mL ethanol/isopropanol, dipping at 35-90 degrees C, drying, heating under water bath at 60-90 degrees C for 4-8 hours to obtain graphene/polyester fabric electrode, performing in-situ chemical polymerization of graphene/polyester fabric electrode with 0.1-0.5 M/L hydrochloric acid/sulfuric acid solution for 1-2 hours at 0-15 degrees C, adding 0.1-0.5 M/L ammonium persulfate, adjusting pH to 0, stirring for 5-90 minutes, and spraying surface. USE - Method for preparing graphene-based and fabric-like polyaniline supercapacitor. ADVANTAGE - The supercapacitor is inexpensive, and has simple preparation and excellent flexibility. DETAILED DESCRIPTION - Preparation of graphene-based and fabric-like polyaniline supercapacitor involves performing chemical reduction of expanded graphite with polyester fabric in 0.5-1 mg/mL ethanol/isopropanol, dipping at 35-90 degrees C, drying, heating under water bath at 60-90 degrees C for 4-8 hours to obtain graphene/polyester fabric electrode, performing in-situ chemical polymerization of graphene/polyester fabric electrode with 0.1-0.5 M/L hydrochloric acid/sulfuric acid solution for 1-2 hours at 0-15 degrees C, adding 0.1-0.5 M/L ammonium persulfate, adjusting pH to 0, stirring for 5-90 minutes, spraying surface in transverse and longitudinal direction with nano silver, and contacting to gel-state electrolyte inside collector grid.