• 专利标题:   Preparing room temperature phosphorescent material containing graphene oxide with microwave radiation comprises using modified Hummers method to oxidize graphite, dissolving acrylamide in water, adding e.g. graphene oxide aqueous solution, mixing, refluxing, cooling, filtering, washing and drying.
  • 专利号:   CN113444194-A, CN113444194-B
  • 发明人:   ZHANG Y, LIN M
  • 专利权人:   UNIV FUJIAN
  • 国际专利分类:   C09K011/02, C09K011/06, C08F002/46, C08K003/04, C08F120/56
  • 专利详细信息:   CN113444194-A 28 Sep 2021 C08F-120/56 202102 Chinese
  • 申请详细信息:   CN113444194-A CN10734997 30 Jun 2021
  • 优先权号:   CN10734997

▎ 摘  要

NOVELTY - Preparing room temperature phosphorescent material containing graphene oxide with microwave radiation comprises firstly using modified Hummers method to oxidize the graphite to obtain graphene oxide, dissolving acrylamide in water, adding graphene oxide aqueous solution and ammonium persulfate dispersed by ultrasonic wave, where the ratio of acrylamide, graphene oxide, ammonium persulfate and water is 100:0.0001-0.002:0.5-1.5:500-2000, mixing uniformly, adding in microwave chemical reactor, refluxing for 3-10 minutes under a microwave output power, cooling, precipitating the obtained product with methanol, filtering, washing the filter cake with methanol and freeze-drying to obtain room temperature phosphorescent material containing graphene oxide with long service life. USE - The method is useful for preparing room temperature phosphorescent material containing graphene oxide with microwave radiation. ADVANTAGE - The method has long phosphorescence life at room temperature; ensures that the luminescence glow reaches after 16 seconds; is simple and convenient; has non-toxic product, no pollution, no heavy metal; is halogen-free; has good water solubility and wide application prospect.