• 专利标题:   Continuous graphene dry-wet combined spinning method involves dispersing large sheets of graphene oxide in water, adding tetrahydrofuran, adding amine organic solvent, spinning, drying, immersing in coagulation bath, drying and processing.
  • 专利号:   CN112030268-A
  • 发明人:   QU J, WANG R, QIAN J, WU M, HU X, MAO Q, JIA W, ZHANG X
  • 专利权人:   UNIV NANTONG
  • 国际专利分类:   D01D001/02, D01D004/02, D01D005/00, D01F009/12
  • 专利详细信息:   CN112030268-A 04 Dec 2020 D01F-009/12 202003 Pages: 6 Chinese
  • 申请详细信息:   CN112030268-A CN10704205 21 Jul 2020
  • 优先权号:   CN10704205

▎ 摘  要

NOVELTY - Continuous graphene dry-wet combined spinning method involves (i) dispersing large sheets of graphene oxide in deionized water, and adding tetrahydrofuran to continue to uniformly disperse, (ii) adjusting viscosity of spinning solution by adding amine organic solvents to form a uniform and stable graphene oxide spinning solution, and (iii) spinning at a uniform speed through spinneret on spinning machine, drying the formed continuous graphene oxide fiber under a tension-free condition with a 450 W infrared lamp for 10 minutes, immersing in a coagulation bath for coordination cross-linking for 1-10 minutes, drying and obtaining graphene fiber through a hydroiodic acid reduction process. USE - Continuous graphene dry-wet combined spinning method. ADVANTAGE - The graphene obtains better flexibility performance while ensuring that the conductivity is not reduced.