• 专利标题:   Preparation of nitrogen-doped graphene quantum dot with high selectivity used for, e.g. detection of hexavalent chromium ion by mixing citric acid and ammonia water, hydrothermally reacting, cooling, heating, dialyzing, and freeze-drying.
  • 专利号:   CN107936964-A
  • 发明人:   ZHANG J, CAI Y, MI C, FAN Y, ZHANG Z, MA Q
  • 专利权人:   UNIV TIANJIN POLYTECHNIC
  • 国际专利分类:   C09K011/65, G01N021/64
  • 专利详细信息:   CN107936964-A 20 Apr 2018 C09K-011/65 201833 Pages: 8 Chinese
  • 申请详细信息:   CN107936964-A CN10890281 13 Oct 2016
  • 优先权号:   CN10890281

▎ 摘  要

NOVELTY - Preparation of nitrogen-doped graphene quantum dot with high selectivity comprises mixing citric acid and ammonia water at volume ratio of 2 g:20 mL to obtain mixed solution, transferring to PTFE-lined reaction kettle, hydrothermally reacting to 160-180 degrees C for 8-12 hours, naturally cooling to room temperature, heating, dialyzing, and freeze-drying. USE - Method for preparation of nitrogen-doped graphene quantum dot with high selectivity used for detection of hexavalent chromium ion (claimed), biological sensor, biological imaging, and high-sensitive fluorescence probe. ADVANTAGE - The product nitrogen-doped graphene quantum dot with high selectivity has low cell toxicity, good biological compatibility, and chromium ion strong detecting effect at detection limit of 50 nM.