• 专利标题:   Preparing nucleus uranium removal adsorbent involves preparaing graphene oxide by mixing graphite, sodium nitrate, and sulfuric acid in beaker and placing in ice bath, and slowly adding potassium permaganate under.
  • 专利号:   CN108620035-A
  • 发明人:   YANG A, ZHU Y, YANG P, LI P, ZHONG J, ZHANG F
  • 专利权人:   CHINA ACAD ENG PHYSICS MATERIAL INST
  • 国际专利分类:   B01J020/24, B01J020/30, C02F001/28, C02F101/20
  • 专利详细信息:   CN108620035-A 09 Oct 2018 B01J-020/24 201872 Pages: 8 Chinese
  • 申请详细信息:   CN108620035-A CN10506549 24 May 2018
  • 优先权号:   CN10506549

▎ 摘  要

NOVELTY - Preparing nucleus uranium removal adsorbent involves preparaing graphene oxide by mixing 2-6 gram graphite, 1-4 gram sodium nitrate, and 85-120 ml sulfuric acid in a beaker and placing in an ice bath, slowly adding 9-15 gram potassium permagnate under continuous stirring, and controlling addition speed to ensure that the temperature of the reaction liquid is not higher than 20 degrees C until the components are completely mixed, removing the ice bath, the temperature of the solution is raised to 30-40 degrees C for 30 minutes, adding 160-200 ml of water, stirring for 30 minutes. 300-500 ml of a solution having hydrogen peroxide concentration of 0.05 wt.% added. The reaction is terminated. The product is a yellow-brown solid, which is centrifuged in a centrifuge and then washed with a concentration of 10% HCL and deionized water for multiple times. USE - Method for preparing nucleus uranium removal adsorbent. ADVANTAGE - The method enables to prepare nucleus uranium removal adsorbent which realizes minimizing of radioactive waste. DETAILED DESCRIPTION - The vacuum environment is used for drying at 40 degrees C to obtain graphene oxide GO, washed the waste tea TW with deionized water multiple times to removed dirt, then boiled in deionized water at 80 degrees C for 1 hours to removed colored and soluble components, then washed with deionized water until colorless, at 100 degrees C dried in an oven, pulverized the obtained product into a powder, and set aside, mixed graphene oxide GO and spare waste tea TW powder in deionized water according to mass ratio 1:1, sonicated for 3 hours, using solid-liquid separation by centrifuge. The separated solid is washed multiple times with deionized water and ethanol, and dried in a vacuum atmosphere at 50 degrees C to obtain final product.