• 专利标题:   Preparing graphene-reinforced resin-based all-carbon composite material comprises e.g. soaking carbon nanotube film in hydrogen peroxide aqueous solution, soaking in aqueous hydrochloric acid solution, and washing using deionized water.
  • 专利号:   CN111747767-A
  • 发明人:   SHEN Y, LEI S, WU G, ZHANG E, SONG Y
  • 专利权人:   UNIV TIANJIN
  • 国际专利分类:   C04B035/524, C04B035/532, C04B035/622, C04B035/626, C04B035/80
  • 专利详细信息:   CN111747767-A 09 Oct 2020 C04B-035/80 202085 Pages: 8 Chinese
  • 申请详细信息:   CN111747767-A CN10699521 20 Jul 2020
  • 优先权号:   CN10699521

▎ 摘  要

NOVELTY - Preparing graphene-reinforced resin-based all-carbon composite material comprises (i) soaking carbon nanotube film in hydrogen peroxide aqueous solution at 50-70 degrees C for 60-72 hours, soaking in aqueous hydrochloric acid solution for 10-12 hours, and washing using deionized water to obtain purified carbon nanotube film, (ii) mechanically uniaxially stretching the purified carbon nanotube film to adjust arrangement direction of carbon nanotubes on the purified carbon nanotube film to be uniform to obtain stretched carbon nanotube film, (iii) soaking the stretched carbon nanotube film in the first liquid for 10-15 minutes to introduce epoxy groups on the surface of the stretched carbon nanotube film, washing the stretched carbon nanotube film with dichloromethane, allowing to stand in a vacuum at 60-80 degrees C to obtain the treated film, where the first liquid is a mixture of meta-chloroperoxybenzoic acid (m-CPBA) and dichloromethane, and m-CPBA in the first liquid is a saturated concentration. USE - The method is useful for preparing graphene-reinforced resin-based all-carbon composite material. ADVANTAGE - The method: slowly solidifies; utilizes the close combination of the soft phase and the hard phase to make the composite material compact; and achieves high thermal conductivity. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is also included for graphene-reinforced resin-based all-carbon composite material obtained by the above preparation method.