• 专利标题:   Method for preparing graphene/long silver nanowire conductive film, involves preparing silver nano line and graphene oxide, adding anionic surfactant, silver nanowire and graphene oxide, followed by filtering, aligning film with substrate.
  • 专利号:   CN107039122-A, CN107039122-B
  • 发明人:   LIU D, ZHANG B, LIANG Y, ZHANG D, TIAN N, ZHANG Y
  • 专利权人:   UNIV BEIJING TECHNOLOGY, UNIV BEIJING TECHNOLOGY
  • 国际专利分类:   H01B013/00
  • 专利详细信息:   CN107039122-A 11 Aug 2017 H01B-013/00 201767 Pages: 9 Chinese
  • 申请详细信息:   CN107039122-A CN10226437 09 Apr 2017
  • 优先权号:   CN10226437

▎ 摘  要

NOVELTY - A graphene/long silver nanowire conductive film preparing method involves preparing silver nano line using polyol method and preparing graphene oxide by Hummers method, adding anionic surfactant into ethylene glycol, followed by adding silver nanowire and graphene oxide to obtain stable suspension. The stable suspension is filtered with hydrazine hydrate to obtain graphene/silver nanowire film. The film is removed from the filter to align the film with a flexible substrate, and placed the aligned substrate in a vacuum oven. The resultant substrate is placed in an acetone and soaked. USE - Method for preparing graphene/long silver nanowire conductive film. ADVANTAGE - The method enables preparing the conductive film with better performance, and transparent and flexible appearance, in a simple, rapid and cost effective manner. DETAILED DESCRIPTION - A graphene/long silver nanowire conductive film preparing method involves preparing silver nano line using polyol method and preparing graphene oxide by Hummers method, adding 1 mg anionic surfactant into 30 ml ethylene glycol, followed by adding 0.15-15 mg silver nanowire and 0.033-3.3 mg graphene oxide to obtain stable suspension. The stable suspension is vacuum-filtered to prepare oxidized graphene/silver nanowire film. The vacuum suction device is kept in a water bath at 90 degrees C and stabilized, followed by filtering the resultant product with 20 ml hydrazine hydrate to obtain graphene/silver nanowire film. The graphene/silver nanowire film is removed from the filter to align the film with a flexible substrate with weight of more than 5 kg, and placed the aligned substrate in a vacuum oven at 60 degrees C for 12 hours. The resultant substrate is placed in an acetone and soaked for 20 minutes and removed to obtain a finished product.