• 专利标题:   Preparing graphene/polylactic acid nano-composite comprises e. g. washing graphene in wet state tetrahydrofuran to remove water content and dissolving polylactic acid graphene in tetrahydrofuran by mechanical stirring.
  • 专利号:   CN110862658-A
  • 发明人:   ZHI T
  • 专利权人:   ZHI T
  • 国际专利分类:   C08K003/04, C08L067/04, G01N023/207, G01N025/00, G01N025/14, G01N003/08, G01N003/40
  • 专利详细信息:   CN110862658-A 06 Mar 2020 C08L-067/04 202023 Pages: 6 Chinese
  • 申请详细信息:   CN110862658-A CN10987532 28 Aug 2018
  • 优先权号:   CN10987532

▎ 摘  要

NOVELTY - Preparing graphene/polylactic acid nano-composite comprises e. g. (i) washing graphene in wet state tetrahydrofuran 5 times to remove water content; (ii) dissolving polylactic acid (1 g graphene corresponds to 4 g polylactic acid) in tetrahydrofuran by mechanical stirring (1 g polylactic acid corresponds to 10 ml tetrahydrofuran); (iii) mechanically stirring in a three-necked flask, dispersing graphite in tetrahydrofuran (1 g graphite dilute corresponds to 40 ml tetrahydrofuran), performing ultrasonic and strong stirring treatment for 2-3 hours until the mixture becomes thick; (iv) adding the polylactic acid solution into the graphite dilute/tetrahydrofuran mixed solution, performing ultrasonic treatment and strong mechanical stirring for 4 hours, pouring the mixture into an open container and drying in an oven at 50 degrees C for 10 hours, making the film on the surface is torn properly, and evaporating the solvent, crushing the resulting film-type solid into particles or powder. USE - The method is useful for preparing graphene/polylactic acid nano-composite. ADVANTAGE - The method is simple and easy to control the temperature. DETAILED DESCRIPTION - Preparing graphene/polylactic acid nano-composite comprises (i) washing graphene in wet state tetrahydrofuran 5 times to remove water content; (ii) dissolving polylactic acid (1 g graphene corresponds to 4 g polylactic acid) in tetrahydrofuran by mechanical stirring (1 g polylactic acid corresponds to 10 ml tetrahydrofuran); (iii) mechanically stirring in a three-necked flask, dispersing graphite in tetrahydrofuran (1 g graphite dilute corresponds to 40 ml tetrahydrofuran), performing ultrasonic and strong stirring treatment for 2-3 hours until the mixture becomes thick; (iv) adding the polylactic acid solution into the graphite dilute/tetrahydrofuran mixed solution, performing ultrasonic treatment and strong mechanical stirring for 4 hours, pouring the mixture into an open container and drying in an oven at 50 degrees C for 10 hours, making the film on the surface is torn properly, evaporating the solvent, crushing the resulting film-type solid into particles or powder, and drying the prepared graphene/polylactic acid nano-composite in a vacuum oven at 80 degrees C for 6 hours; and (v) performing performance test on the obtained product.