• 专利标题:   Hydrothermal synthesis of oxygen and chlorine co-doped graphene quantum dot involves adding sugar aqueous solution with hydrochloric acid to react, cooling reaction liquid to room temperature, and carrying out dialysis purification.
  • 专利号:   CN103359727-A, CN103359727-B
  • 发明人:   LI X, TANG L, YANG P, YANG W
  • 专利权人:   UNIV YUNNAN NORMAL
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN103359727-A 23 Oct 2013 C01B-031/04 201403 Pages: 10 Chinese
  • 申请详细信息:   CN103359727-A CN10312836 24 Jul 2013
  • 优先权号:   CN10312836

▎ 摘  要

NOVELTY - Hydrothermal synthesis of oxygen and chlorine co-doped graphene quantum dot is carried out by dissolving sugar as carbon source and oxygen doping source into water to obtain 0.1-15 wt.% sugar aqueous solution; adding sugar aqueous solution with hydrochloric acid and reacting at 120-220 degrees C for 0.5-10 hours, where mole ratio of carbon in sugar to hydrochloric acid is 5:1-1:10; and after the reaction is finished, cooling the reaction liquid to room temperature, and carrying out dialysis purification to obtain oxygen and chlorine co-doped graphene quantum dot. USE - Method for hydrothermal synthesis of oxygen and chlorine co-doped graphene quantum dot (claimed). ADVANTAGE - The method can increase graphene quantum dot electronic transition level by introducing oxygen and chlorine, and the prepared co-doped graphene quantum dot has excellent light emitting property.