• 专利标题:   Method for preparing electric sensor material for detecting cadmium ion, lead ion, copper ion and manganese ion, involves preparing graphene oxide, adding ferric chloride hexahydrate and terephthalic acid to N,N-dimethylformamide solution.
  • 专利号:   CN110646477-A
  • 发明人:   JIANG H, CHEN J, CHEN P, ZHU T, CAO Q, LIU Z, DAI Y, JIANG W, DENG C
  • 专利权人:   UNIV NANCHANG HANGKONG
  • 国际专利分类:   G01N027/26
  • 专利详细信息:   CN110646477-A 03 Jan 2020 G01N-027/26 202007 Pages: 6 Chinese
  • 申请详细信息:   CN110646477-A CN10914647 26 Sep 2019
  • 优先权号:   CN10914647

▎ 摘  要

NOVELTY - An electric sensor material preparing method involves preparing graphene oxide by utilizing conventionally reported methods, slowly adding a certain amount of ferric chloride hexahydrate and terephthalic acid to 50 mL of N, N-dimethylformamide solution, stirring the solution at room temperature for 30 minutes to obtain a clear and transparent mixed solution A, adding graphene oxide to the mixed solution A under the mass ratio of graphene oxide to the amount of ferric chloride hexahydrate substance is 1: 0.5-1: 2000, ultrasonically dispersing the solution for 20 minutes, stirring and dispersing for 30 minutes, and transferring the obtained mixed solution to a reaction kettle for solvothermal reaction under the reaction temperature at 100-180 degrees C, and the reaction time for 4-14 hours, after the reaction, cooling to room temperature, collecting the product, washing and drying to obtain the final product. USE - Method for preparing electric sensor material for detecting cadmium ion, lead ion, copper ion and manganese ion. ADVANTAGE - The method enables preparing electric sensor material with high detection sensitivity, better stability and strong anti-interference performance, in simple preparation method and cost effective manner. DETAILED DESCRIPTION - An electric sensor material preparing method involves preparing graphene oxide by utilizing conventionally reported methods, slowly adding a certain amount of ferric chloride hexahydrate and terephthalic acid to 50 mL of N, N-dimethylformamide solution under the amount of ferric chloride hexahydrate ranges from 1-20 mmol and the amount of terephthalic acid is 1-20 mmol, stirring the solution at room temperature for 30 minutes to obtain a clear and transparent mixed solution A, adding graphene oxide to the mixed solution A under the mass ratio of graphene oxide to the amount of ferric chloride hexahydrate substance is 1: 0.5-1: 2000, ultrasonically dispersing the solution for 20 minutes, stirring and dispersing for 30 minutes, and transferring the obtained mixed solution to a reaction kettle for solvothermal reaction under the reaction temperature at 100-180 degrees C, and the reaction time for 4-14 hours, after the reaction, cooling to room temperature, collecting the product, washing and drying to obtain the final product.