• 专利标题:   Preparing graphene involves taking graphene oxide in sample vial, adding deionized water and then placing vial in ultrasonic cleaner to obtain yellow-brown oxide graphene dispersion.
  • 专利号:   CN105948022-A
  • 发明人:   PENG L, YU H, ZHENG Y
  • 专利权人:   NINGBO ZHONGKE JIANHUA NEW MATERIAL CO
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN105948022-A 21 Sep 2016 C01B-031/04 201676 Pages: 8 Chinese
  • 申请详细信息:   CN105948022-A CN10264703 26 Apr 2016
  • 优先权号:   CN10264703

▎ 摘  要

NOVELTY - Preparing graphene involves taking the graphene oxide in a sample vial, adding deionized water and then placing the vial in an ultrasonic cleaner for 30 min to obtain a yellow-brown oxide graphene dispersion. The pyrocatechol is added into the graphene dispersion solution and the pyrocatechol is fully dissolved by continuous stirring to obtain the mixed solution, where the amount of pyrocatechol is 1-10 wt.% of the total mass of the graphene oxide. The vial containing the mixed solution is heated in an oven to obtain a black dispersion. USE - Method for preparing graphene (claimed). ADVANTAGE - The method enables to prepare graphene, that has low energy consumption, high efficiency, good stability, can be stored for a long time, is safe, non-toxic and conductive. DETAILED DESCRIPTION - Preparing graphene involves taking the graphene oxide in a sample vial, adding deionized water and then placing the vial in an ultrasonic cleaner for 30 min to obtain a yellow-brown oxide graphene dispersion. The pyrocatechol is added into the graphene dispersion solution and the pyrocatechol is fully dissolved by continuous stirring to obtain the mixed solution, where the amount of pyrocatechol is 1-10 wt.% of the total mass of the graphene oxide. The vial containing the mixed solution is heated in an oven to obtain a black dispersion. The resulting black dispersion is filtered, washed and dried in vacuum to give the product, and the product is characterized.