• 专利标题:   Preparing catalyst useful for catalytic synthesis of imine, comprises dispersing fluorinated graphene in deionized water ultrasonically, adding sodium molybdate and L-cysteine dissolved solution, ultrasonicating, reacting in hydrothermal kettle, centrifuging, filtering, washing and drying.
  • 专利号:   CN115055193-A
  • 发明人:   ZHU Y, ZHANG J
  • 专利权人:   NANJING GUOFENG NEW MATERIAL TECHNOLOGY CO LTD
  • 国际专利分类:   B01J027/051, C07C249/02, C07C251/24
  • 专利详细信息:   CN115055193-A 16 Sep 2022 B01J-027/051 202295 Chinese
  • 申请详细信息:   CN115055193-A CN10633381 06 Jun 2022
  • 优先权号:   CN10633381

▎ 摘  要

NOVELTY - Preparing catalyst comprises (i) dissolving the sodium molybdate and L-cysteine in the deionized water and stirring to dissolve completely to obtain a solution; (ii) dispersing the fluorinated graphene into the deionized water, dispersing ultrasonically and completely, adding the obtained solution and ultrasonicating continuously for 10-20 minutes; and (iii) transferring the mixture obtained into the hydrothermal kettle, reacting for 20-28 hours at 120-300℃, centrifuging, filtering, washing with absolute ethyl alcohol and drying for 8-16 hours at 60-100℃. USE - The method is useful for preparing catalyst is useful for catalytic synthesis of imine. ADVANTAGE - The method: has simple steps and mild reaction conditions; and is economical.