• 专利标题:   Preparing graphene powder by rapid macromolecule reduction comprises adopting the improved Hummers method to obtain graphite oxide, diluting, ultrasonically oscillation, stirring, reacting drying, crushing and sieving.
  • 专利号:   CN106957053-A
  • 发明人:   MA L, XIAO S, WANG L, WANG Y, ZHAO C, XUE J, ZHU S, SONG X, WANG C
  • 专利权人:   SHANDONG YUHUANG NEW ENERGY TECHNOLOGY
  • 国际专利分类:   C01B032/184
  • 专利详细信息:   CN106957053-A 18 Jul 2017 C01B-032/184 201760 Pages: 8 Chinese
  • 申请详细信息:   CN106957053-A CN10239803 13 Apr 2017
  • 优先权号:   CN10239803

▎ 摘  要

NOVELTY - Preparing graphene powder by rapid macromolecule reduction comprises (a) adopting the improved Hummers method to obtain graphite oxide, using pure water for diluting the oxidation product, ultrasonically oscillation or strong stirring process to obtain oxidized graphene acid solution, (b) transferring the oxidized graphene solution into the reaction container, raising the temperature to 40-98 degrees C, under the condition of stirring, adding reducing iron powder, reacting for 1-6 hours, allowing to stand and cooling to 50 degrees C, filtering when it is hot, washing, drying, crushing and sieving. USE - The method is useful for preparing graphene powder by rapid macromolecule reduction (claimed). ADVANTAGE - The method is economical, has no toxicity, is environmentally friendly, requires low energy consumption and suitable for large-scale production.