• 专利标题:   Preparation of antibacterial material by pretreating diatomaceous earth, dropwise adding silver nitrate solution into graphene oxide under magnetic stirring condition, ultrasonically processing, centrifuging and ultrasonically processing.
  • 专利号:   CN108684708-A
  • 发明人:   GAO L, WANG L, ZHAO Y, SHI N, WANG F, WANG H, GUO J, YANG L, SONG Y
  • 专利权人:   UNIV NORTH CHINA
  • 国际专利分类:   A01N025/08, A01N059/00, A01N059/16, A01P001/00
  • 专利详细信息:   CN108684708-A 23 Oct 2018 A01N-059/16 201881 Pages: 12 Chinese
  • 申请详细信息:   CN108684708-A CN10788318 18 Jul 2018
  • 优先权号:   CN10788318

▎ 摘  要

NOVELTY - Preparation of antibacterial material comprises pretreating diatomaceous earth (DE), preparing silver-loaded graphene oxide (Ag+-GO) by dropwise adding 0.1 mol/L silver nitrate solution into 1 mg/ml GO under magnetic stirring condition, where volume ratio of GO and AgNO3 solution is 1:1 and silver ions are uniformly combined on GO sheet, ultrasonically processing at 180 W and 60 kHz for 30 minutes, centrifuging at 13000 revolutions/minute, ultrasonically processing at 180 W and 60 kHz for 2 hours, dispersing in deionized water to obtain Ag+-GO dispersion and storing at 4 degrees C, preparing Ag+-GO/DE by weighing 10 g pretreated DE, adding 20 ml Ag+-GO dispersion, preparing into paste, oven drying at 70 degrees C, grinding and sieving by 100-mesh sieve, and preparing silver nanoparticle (AgNP)/GO/DE by dry grinding Ag+-GO/DE, adding to 50 ml of 0.2 mol/L sodium borohydride solution, magnetically stirring for 1 hour, oven drying at 70 degrees C, grinding and sieving by 100-mesh sieve. USE - Preparation of antibacterial material i.e. AgNP/GO/DE (claimed). ADVANTAGE - The method improves the adsorption capacity and antibacterial ability of DE, solves the safety problem of AgNP-GO, improves the sustained release property of nano-silver, has simple steps and low cost, and is easy for mass production.