• 专利标题:   Preparation of independent self-supporting artificial nano-graphite film used e.g. in nanomaterial, by mixing graphene oxide and graphitizable macromolecule, coating on substrate, heating and making substrate surface having volatile coating.
  • 专利号:   CN111547716-A
  • 发明人:   WANG L, FANG X, WANG J
  • 专利权人:   TIANJIN DANCONG NEW MATERIAL TECHNOLOGY CO LTD
  • 国际专利分类:   C01B032/205
  • 专利详细信息:   CN111547716-A 18 Aug 2020 C01B-032/205 202074 Pages: 8 Chinese
  • 申请详细信息:   CN111547716-A CN10566967 19 Jun 2020
  • 优先权号:   CN10566967

▎ 摘  要

NOVELTY - An independent self-supporting artificial nano-graphite film is prepared by mixing graphene oxide and graphitizable macromolecule, coating on substrate, forming film, performing heat treatment to 400-600 degrees C at 1-10 degrees C/minute, maintaining for 1-4 hours, heating under vacuum to 700-1600 degrees C at 1-10 degrees C/minute, maintaining for 0.1-2 hours, heating to 2000-2300 degrees C at 1-20 degrees C/minute, maintaining for 2-4 hours, heating to 2800-3200 degrees C for 0.5-2 hours at 1-20 degrees C/minute, and making substrate surface having volatile coating. The thickness of artificial nano-graphite film is 100-280 nm. The volatile coating is polycrystalline nano-coating that can volatilize or decompose at 700-1600 degrees C, and has thickness of less than or equal to 20 nm. USE - The method is used for preparing independent self-supporting artificial nano-graphite film in nanomaterial including heat conductivity, electrical conductivity, light absorption and drug detection. ADVANTAGE - The film has flat surface, uniform thickness structure, controllable horizontal size and vertical thickness and no layering phenomenon on vertical direction.