• 专利标题:   Preparation of vanadium tetrasulfide/graphene composite material for sodium ion battery electrode involves dissolving graphene oxide in deionized water, and ultrasonically dispersing to form graphene oxide solution.
  • 专利号:   CN108598432-A
  • 发明人:   LIAO J, WANG S, WU M, XU Z, GONG F, FENG T
  • 专利权人:   UNIV CHINA ELECTRONIC SCI TECHNOLOGY
  • 国际专利分类:   B82Y030/00, H01M010/054, H01M004/36, H01M004/58, H01M004/62
  • 专利详细信息:   CN108598432-A 28 Sep 2018 H01M-004/36 201874 Pages: 9 Chinese
  • 申请详细信息:   CN108598432-A CN10409097 02 May 2018
  • 优先权号:   CN10409097

▎ 摘  要

NOVELTY - The preparation of vanadium tetrasulfide/graphene composite material for sodium ion battery electrode, involves dissolving graphene oxide in deionized water, ultrasonically dispersing to form graphene oxide solution, adding vanadium source and sulfur source to graphene oxide solution according to vanadium and sulfur molar ratio of (0.95-1.05):(4.95-5.05), stirring for 0.5-6 hours to form mixed solution, transferring the mixed solution to the inner tank of the reaction vessel, hydrothermally reacting at 140-240 degrees C for 12-48 hours, cooling the reaction vessel to room temperature, washing the obtained product and drying. The concentration of graphene oxide is 0.3-30 mg/ml. USE - Preparation of vanadium tetrasulfide/graphene composite material for sodium ion battery electrode. ADVANTAGE - The method enables preparation of vanadium tetrasulfide/graphene composite material with high repeatability by simple and economical process, effectively improves the electrical conductivity of the composite electrode material, improves high rate characteristics and cycle stability, and achieves high large current charge and discharge capacity of battery.