• 专利标题:   Using cellulosic polymer to provide concentrated graphene for preparing graphene ink composition, comprises e.g. exfoliating graphene source material with medium comprising organic solvent and dispersing agent comprising cellulosic polymer.
  • 专利号:   US2018340090-A1
  • 发明人:   HERSAM M C, LIANG Y T
  • 专利权人:   UNIV NORTHWESTERN
  • 国际专利分类:   C08K005/05, C09D101/28
  • 专利详细信息:   US2018340090-A1 29 Nov 2018 C09D-101/28 201882 Pages: 15 English
  • 申请详细信息:   US2018340090-A1 US042251 23 Jul 2018
  • 优先权号:   US478361P, US042251

▎ 摘  要

NOVELTY - Using a cellulosic polymer to provide concentrated graphene in preparation of a graphene ink composition, comprises: exfoliating a graphene source material with a medium comprising an organic solvent at least partially miscible with water and a dispersing agent comprising a cellulosic polymer at least partially soluble in the organic solvent, where the graphene source material is not oxidized; contacting at least a portion of the exfoliated graphene medium with a hydrophobic fluid component; and hydrating the exfoliated graphene medium to concentrate the exfoliated graphene in the hydrophobic fluid component, where the concentrated graphene medium is achieved without application of centrifugal force. USE - The method is useful for preparation of the graphene ink composition. ADVANTAGE - The method is rapid, scalable and economical; is carried out without centrifugation, and thus enhances graphene concentration; utilizes low-cost organic solvents otherwise deemed ineffective for purposes of graphene exfoliation and/or dispersion.