• 专利标题:   Composite material used in hydrogen-storage application, comprises graphene sheet and cobalt sulfide adhered to surface of graphene sheet.
  • 专利号:   CN104229731-A, CN104229731-B
  • 发明人:   HAN L, GANG P, QIN W
  • 专利权人:   HARBIN INST TECHNOLOGY, HARBIN INST TECHNOLOGY
  • 国际专利分类:   C01B003/02, C01B031/04, C01G051/00
  • 专利详细信息:   CN104229731-A 24 Dec 2014 C01B-003/02 201522 Pages: 9 Chinese
  • 申请详细信息:   CN104229731-A CN10471800 16 Sep 2014
  • 优先权号:   CN10471800

▎ 摘  要

NOVELTY - A composite material comprises graphene sheet and cobalt sulfide adhered to a surface of graphene sheet, and has layered structure. The molar ratio of graphene and cobalt sulfide is 1:(5-7). USE - Composite material is used in hydrogen-storage application (claimed). ADVANTAGE - The composite material has maximum hydrogen storage capacity of 3.73 wt.% or less. DETAILED DESCRIPTION - An INDEPENDENT CLAIM is included for preparation of composite material, which involves mixing cobalt powder and sulfur powder in molar ratio of 1:(0.9-1.1), obtaining mixed powder (a), mixing zirconia balls and the mixed powder (a) in mass ratio of (10-15):1, ball milling in a ball milling tank for 8-12 hours in high-pure argon gas atmosphere at 600-800 rpm, cooling the resultant material to room temperature, obtaining cobalt sulfide powder, adding graphene, mixing uniformly, obtaining mixed powder (b), mixing zirconia balls with mixed powder (b) in mass ratio of (15-20):1, ball milling in a ball milling tank for 8-12 hours in high-pure argon gas atmosphere at 600-800 rpm and cooling the resultant material to room temperature.