• 专利标题:   Producing graphene, comprises e.g. treating crystalline graphite with ammonium persulfate solution in sulfuric acid which is free of water, holding the resulting intercalated graphite compound before expansion, and performing hydrolysis.
  • 专利号:   RU2016137248-A, RU2657504-C2
  • 发明人:   TKACHEV A G, MELEZHIK A V, MEMETOV N R, OSIPOV A A
  • 专利权人:   NANOTEKHTSENTR LTD, NANOTEKHTSENTR CO LTD
  • 国际专利分类:   C01B032/192, B82B003/00, B82Y040/00
  • 专利详细信息:   RU2016137248-A 19 Mar 2018 C01B-032/192 201829 Pages: 1 Russian
  • 申请详细信息:   RU2016137248-A RU137248 16 Sep 2016
  • 优先权号:   RU137248

▎ 摘  要

NOVELTY - Producing graphene, comprises treating crystalline graphite with a solution of ammonium persulfate in sulfuric acid containing no free water, holding the resulting intercalated graphite compound before expansion, performing hydrolysis and washing with water, and carrying out ultrasonic dispersion in an aqueous surfactant solution, where the surfactant is a mixture of oligomeric compounds containing cumulative double carbon-carbon bonds and amino groups (aminocumulene) at a pH of an aqueous solution of greater than or equal to 6 and a weight ratio of aminocumulene:graphene is 0.25:1-4:1. USE - The process is useful for producing graphene.