▎ 摘　　要

NOVELTY - The method comprises (i) taking monodisperse colloidal nano-particles with different sizes as an assembling unit, combining the two kinds of nanoparticles with effective particle diameter ratio, uniformly mixing according to the ratio of the chemical quantity, preparing a binary super-crystal by the co-assembly method, (ii) controlling the temperature of the in-situ ligand carbonization, crosslinking and carbonizing the organic molecular ligand of the binary supercrystal surface obtained in the step (1), (iii) using acid solution to etch the remove obtained in step (2) on the surface to obtain the redundant nanoparticles, (iv) selecting proper graphitization temperature to ensure that the ordered double mesophorous carbon skeleton is stable, and (v) realizing graphitizing of the carbon layer at the same time. USE - Preparation method for ordered double mesoporous carbon graphene material or ordered double mesoporous carbon material used in sensor piece bioreactor and energy storage and conversion field. ADVANTAGE - The ordered double-mesoporous carbon material has rich and adjustable multi-hole stacking structure, excellent conductivity of the graphite and ultra-high specific surface area of the multi-stage hole. DESCRIPTION OF DRAWING(S) - The drawing shows a schematic representation of the preparation method for ordered double mesoporous carbon graphene material or ordered double mesoporous carbon material.