• 专利标题:   Preparing graphene involves dispersing graphite in solution of sodium bicarbonate, heating resulting product, maintaining constant temperature, ultrasonically vibrating; adding sodium hydroxide solution, and regulating pH value.
  • 专利号:   CN103950928-A, CN103950928-B
  • 发明人:   JIN C, YANG X
  • 专利权人:   SUZHOU SDIK NEW MATERIAL TECHNOLOGY CO, SUZHOU SIDIKE NEW MATERIALS SCI TECHNO
  • 国际专利分类:   C01B031/04
  • 专利详细信息:   CN103950928-A 30 Jul 2014 C01B-031/04 201468 Pages: 9 Chinese
  • 申请详细信息:   CN103950928-A CN10219485 22 May 2014
  • 优先权号:   CN10219485

▎ 摘  要

NOVELTY - Preparing graphene involves dispersing graphite in a solution of sodium bicarbonate, at 80-150 degrees C, under a degree of vacuum 0-1000 Pa, heating resulting product to 130-270 degrees C, maintaining constant temperature for 5-48 hours; ultrasonically vibrating for 30-1 hours; adding sodium hydroxide solution, regulating pH value to 7.8-10, standing for 24-72 hours to obtain suspension, at 60-100 degrees C, drying for 12-24 hours. USE - For preparing graphene (claimed). ADVANTAGE - The reaction a temperature control at 500 degrees C, which is good for preparation table with a larger area than a grapheme. The method avoids agglomeration, and does not need to add stabilizing agent.