• 专利标题:   Preparation of gold-reduced graphene oxide-nickel foam composite, involves immersing graphene oxide-nickel foam in aqueous solution of ascorbic acid, immersing reduced graphene oxide-nickel foam material in chloroauric acid solution.
  • 专利号:   CN107354336-A, CN107354336-B
  • 发明人:   GUO X, LIU Y, LIU C, ZHU L, WANG X, ZHAO L, GE C, ZHANG W
  • 专利权人:   UNIV SOUTHEAST, UNIV SOUTHEAST
  • 国际专利分类:   B22F009/24, B82Y040/00, C01B032/184, C22C001/08
  • 专利详细信息:   CN107354336-A 17 Nov 2017 C22C-001/08 201781 Pages: 8 Chinese
  • 申请详细信息:   CN107354336-A CN10578823 14 Jul 2017
  • 优先权号:   CN10578823

▎ 摘  要

NOVELTY - Preparation of gold-reduced graphene oxide-nickel foam composite, involves dispersing graphene oxide in deionized water to form graphene oxide aqueous solution, immersing nickel foam in graphene oxide aqueous solution to obtain graphene oxide-nickel foam, immersing graphene oxide-nickel foam in aqueous solution of ascorbic acid to obtain reduced graphene oxide-nickel foam material, immersing reduced graphene oxide-nickel foam material in chloroauric acid solution, carrying out exchange reaction between trivalent gold ions and substrate nickel to obtain final product. USE - Method for preparing gold-reduced graphene oxide-nickel foam composite (claimed). DETAILED DESCRIPTION - Method for preparing gold-reduced graphene oxide-nickel foam composite, involves (1) dispersing graphene oxide in deionized water, forming 0.5-2 mg/mL concentration of graphene oxide aqueous solution, (2) ultrasonically cleaning nickel foam with acetone, ethanol and deionized water, drying, immersing nickel foam in graphene oxide aqueous solution, removing and drying, repeatedly immersing in graphene oxide aqueous solution, drying for several times to obtain graphene oxide-nickel foam, (3) immersing graphene oxide-nickel foam in aqueous solution of ascorbic acid with concentration of 10/3-10 mg/ml, heating to obtain reduced graphene oxide-nickel foam material, (4) immersing reduced graphene oxide-nickel foam material in solution of chloroauric acid with concentration of 5-10 mmol/l, ultrasonically processing, carrying out exchange reaction between trivalent gold ions and substrate nickel to obtain final product.