• 专利标题:   Synthesis of 3-aminopropyltriethoxysilane-modified graphene oxide by adding graphene oxide into water, ultrasonically dispersing, adding 3-aminopropyltriethoxysilane and catalyst, and stirring to react.
  • 专利号:   CN107746054-A
  • 发明人:   WANG Y, WANG W, DING F, JI Y, CHEN B, GAO F, ZHU Y, YAN Z
  • 专利权人:   XI AN MODERN CHEM RES INST
  • 国际专利分类:   C01B032/198
  • 专利详细信息:   CN107746054-A 02 Mar 2018 C01B-032/198 201825 Pages: 5 Chinese
  • 申请详细信息:   CN107746054-A CN11107602 10 Nov 2017
  • 优先权号:   CN11107602

▎ 摘  要

NOVELTY - Synthesis of 3-aminopropyltriethoxysilane-modified graphene oxide using graphene oxide as raw material comprises adding graphene oxide into water, ultrasonically dispersing, adding 3-aminopropyltriethoxysilane and catalyst, where mass ratio of graphene oxide, water, 3-aminopropyltriethoxysilane and catalyst is 1.0-3.0:800-1200:5.0-10.0:0.5-3.0, stirring to react at 30-45 degrees C for 0.5-1.5 hours, centrifuging, washing and drying to obtain black powder i.e. 3-aminopropyltriethoxysilane-modified graphene oxide. The catalyst is 10 mass% hydrochloric acid or 10 mass% sulfuric acid. USE - Synthesis of 3-aminopropyltriethoxysilane-modified graphene oxide using graphene oxide as raw material. ADVANTAGE - The method solves the prior art problem of long reaction time and the use of organic solvent. DETAILED DESCRIPTION - Synthesis of 3-aminopropyltriethoxysilane-modified graphene oxide using graphene oxide as raw material comprises adding graphene oxide into water, ultrasonically dispersing at 25-35 degrees C for 0.3-1.2 hours, adding 3-aminopropyltriethoxysilane and catalyst, where mass ratio of graphene oxide, water, 3-aminopropyltriethoxysilane and catalyst is 1.0-3.0:800-1200:5.0-10.0:0.5-3.0, stirring to react at 30-45 degrees C for 0.5-1.5 hours, centrifuging, washing and drying to obtain black powder i.e. 3-aminopropyltriethoxysilane-modified graphene oxide. The catalyst is 10 mass% hydrochloric acid or 10 mass% sulfuric acid.