• 专利标题:   Preparing rGO-PTCA-RhB composite material comprises e.g. ultrasonically dispersing graphene oxide in deionized water, adding 3,4,9,10-decanetetracarboxylic acid, reducing agent and aqueous ammonia and dissolving rGO-PTCA in deionized water.
  • 专利号:   CN109911891-A
  • 发明人:   MO Z, YANG X, NIU X, ZHAO P, LIU Z, GUO R, LIU N
  • 专利权人:   UNIV NORTHWEST NORMAL
  • 国际专利分类:   C01B032/194, C01B032/198
  • 专利详细信息:   CN109911891-A 21 Jun 2019 C01B-032/198 201973 Pages: 6 Chinese
  • 申请详细信息:   CN109911891-A CN10124193 19 Feb 2019
  • 优先权号:   CN10124193

▎ 摘  要

NOVELTY - Preparing rGO-PTCA-RhB composite material comprises (i) rGO-PTCA is obtained by ultrasonically dispersing graphene oxide in deionized water to form a uniform suspension, adding 3,4,9,10-decanetetracarboxylic acid to the suspension, stirring evenly, adding reducing agent and aqueous ammonia solution, stirring at 90-95 degrees C for 2-3 hours, allowing to stand for 30-40 minutes, separating, washing and drying, and (ii) rGO-PTCA-RhB composite is obtained by dissolving rGO-PTCA in deionized water, ultrasonizing for 3-5 hours, adding ethylenediamine and rhodamine B, stirring evenly and adding crosslinker EDC and NHS, reacting at room temperature for 22-24 hours, filtering and drying. USE - The methods is useful for preparing rGO-PTCA-RhB composite material. ADVANTAGE - The material has good conductivity and has good the electrochemical field.