• 专利标题:   Preparing molybdenum disulfide nanosheet composite graphene for electrochemical energy storage, by adding molybdenum source to water, adding sulfur source to water, dispersing graphene, mixing, reacting, cooling, centrifuging and drying.
  • 专利号:   CN112225210-A
  • 发明人:   MENG Z, ZHENG G, LONG F, WANG J
  • 专利权人:   UNIV GUILIN TECHNOLOGY
  • 国际专利分类:   B82Y030/00, B82Y040/00, C01B032/194, C01G039/06
  • 专利详细信息:   CN112225210-A 15 Jan 2021 C01B-032/194 202117 Pages: 7 Chinese
  • 申请详细信息:   CN112225210-A CN11080780 11 Oct 2020
  • 优先权号:   CN11080780

▎ 摘  要

NOVELTY - Method for preparing molybdenum disulfide nanosheet composite graphene, involves (i) adding molybdenum source to water to obtain a solution (A), (ii) adding sulfur source to water to obtain a solution (B), (iii) dispersing graphene in water to form a solution (C), (iv) mixing the solutions (A), (B) and (C), completely stirring, transferring to an 80 ml PTFE high pressure reaction kettle for sealing, transferring the reaction kettle to an oven, setting the temperature at 160-200 degrees C and reacting for 12-24 hours, and cooling to room temperature to obtain a suspension, and (v) centrifuging and washing the suspension obtained in step (iv) with deionized water for 5-6 times, and drying the centrifugal product in a freeze-dryer to obtain the molybdenum disulfide composite graphene material powder. USE - The method is useful for preparing molybdenum disulfide nanosheet composite graphene for electrochemical energy storage. ADVANTAGE - The method uses simple equipment and low raw material price, and has non-toxicity.