• 专利标题:   Preparing titanium-doped graphene-coated lithium iron phosphate cathode material, comprises e.g. mixing and dispersing graphene oxide and titanium carbide-MXene etching dispersion liquid in solvent, adding lithium source, iron source and phosphorus source, sintering and crushing.
  • 专利号:   CN115676814-A
  • 发明人:   DENG Q, FAN S, WANG Z, QIN H, HU Z, ZHANG C, ZHENG L, SHEN W, LUO B, WANG D
  • 专利权人:   YIDU XINGFA CHEM CO LTD
  • 国际专利分类:   C01B025/45, C01B032/19, C01B032/194, C01G023/047, H01M004/36, H01M004/38, H01M004/58
  • 专利详细信息:   CN115676814-A 03 Feb 2023 C01B-032/19 202323 Chinese
  • 申请详细信息:   CN115676814-A CN11376879 04 Nov 2022
  • 优先权号:   CN11376879

▎ 摘  要

NOVELTY - Preparing titanium-doped graphene-coated lithium iron phosphate cathode material, comprises (i) mixing and dispersing graphene oxide and titanium carbide (Ti3C2)-MXene etching dispersion liquid in a solvent in an ice bath, and ultrasonically dispersing, (ii) adding lithium source, iron source, and phosphorus source to the dispersion liquid in sequence, adding water to dilute, stirring and carrying out ultrasonic dispersion in ice bath again, (iii) transferring the mixture solution into a polytetrafluoroethylene reactor for hydrothermal reaction to obtain the mixture aerogel, (iv) washing the mixture aerogel alternately with deionized water and ethanol, and freeze-drying to obtain a precursor, and (v) placing the dried precursor in a tube furnace with a protective atmosphere, sintering and crushing. USE - The method is useful for preparing titanium-doped graphene-coated lithium iron phosphate cathode material. ADVANTAGE - The method realizes titanium doping and graphene coating of lithium iron phosphate, is simple and effective, and improves the intrinsic conductivity and ion diffusion kinetics of lithium iron phosphate.