• 专利标题:   Preparing a graphene comprises e.g. taking graphite, potassium permanganate and sulfuric acid and mixing uniformly, stirring while reacting, adding water, hydrogen peroxide solution, stirring reacting and performing solid-liquid separation.
  • 专利号:   CN108017052-A
  • 发明人:   LIANG Y, CHEN G, YANG Z, ZHU H
  • 专利权人:   GUANGDONG POLYROCKS CHEM CO LTD
  • 国际专利分类:   C01B032/19
  • 专利详细信息:   CN108017052-A 11 May 2018 C01B-032/19 201841 Pages: 7 Chinese
  • 申请详细信息:   CN108017052-A CN11190738 24 Nov 2017
  • 优先权号:   CN11190738

▎ 摘  要

NOVELTY - Preparing a graphene comprises (i) taking graphite, potassium permanganate and sulfuric acid and mixing uniformly, stirring while reacting at 0-100 degrees C for 10-120 minutes, adding water and hydrogen peroxide solution, stirring while reacting for 1-15 minutes and performing solid-liquid separation to obtain intercalated graphite; and (ii) dispersing the intercalated graphite in water and placing in a microwave reactor, charging with protective gas, performing microwave reaction for 1-15 minutes and performing solid-liquid separation. USE - The method is useful for preparing a graphene. ADVANTAGE - The method produces graphene in large scale, has simple process, short flow, mild reaction conditions, low cost, easy mass production, excellent graphene performance, less structural defects and has good quality stability between batches.