• 专利标题:   Preparing graphene loaded carbon-coated lithium vanadium phosphate composite material used as a lithium ion cathode material comprises performing modified Hummers method, sol-gel method, microwave digestion, pre-sintering and sintering.
  • 专利号:   CN110518215-A
  • 发明人:   WANG Q, HE D, ZHANG W, LIU H, KAN K, WANG J, YU Q
  • 专利权人:   HEILONGJIANG ACAD SCI ADVANCED TECHNOLOG
  • 国际专利分类:   H01M010/0525, H01M004/36, H01M004/58, H01M004/62
  • 专利详细信息:   CN110518215-A 29 Nov 2019 H01M-004/36 201996 Pages: 12 Chinese
  • 申请详细信息:   CN110518215-A CN10825093 02 Sep 2019
  • 优先权号:   CN10825093

▎ 摘  要

NOVELTY - Preparing graphene loaded carbon-coated lithium vanadium phosphate composite material comprises (a) using expanded graphite as raw material and preparing graphene oxide by a modified Hummers method, (b) using the carbon-coated lithium vanadium phosphate precursor prepared by sol-gel method, (c) using microwave digestion method to prepare graphene/carbon coated lithium vanadium phosphate precursor and (d) pre-sintering and sintering under the protection of nitrogen. USE - The material is useful as lithium ion cathode material. ADVANTAGE - The material: has a specific discharge capacity of 130 mAh/g; has a voltage range of 3-4.3 V at a rate of 0.5C; reaches a specific capacity retention rate of 99.5%, when it is cycled for 100 weeks at a rate of 0.5 C.