• 专利标题:   Preparing modified graphene flakes by using thermal decomposition of precursor of titanium dioxide produced from organotitanium compound, comprises e.g. dispersing flakes of graphene or graphene oxide in organic solvent.
  • 专利号:   PL411393-A1, PL226568-B1
  • 发明人:   JURECZKO J, KURNICKI A, JASTRZEBSKA A, OLSZYNA A
  • 专利权人:   POLITECHNIKA WARSZAWSKA, POLITECHNIKA WARSZAWSKA
  • 国际专利分类:   B82Y040/00, C01B031/00, C01G023/047, B01J021/06, B01J021/18
  • 专利详细信息:   PL411393-A1 29 Aug 2016 C01B-031/00 201669 Pages: 1
  • 申请详细信息:   PL411393-A1 PL411393 26 Feb 2015
  • 优先权号:   PL411393

▎ 摘  要

NOVELTY - Preparing modified graphene flakes by using thermal decomposition of precursor of titanium dioxide produced from organotitanium compound, comprises dispersing flakes of graphene or graphene oxide in an organic solvent comprising aliphatic hydrocarbons containing 3-9 carbons, adding organotitanium compounds (I)-(IV) and/or (V), then stirring in the presence of a dry or humid air, removing the solvent and the residue, and after drying, decomposing thermally to air at 200-700 degrees C. USE - The method is useful for preparing modified graphene flakes. DETAILED DESCRIPTION - Preparing modified graphene flakes by using thermal decomposition of precursor of titanium dioxide produced from organotitanium compound, comprises dispersing flakes of graphene or graphene oxide in an organic solvent comprising aliphatic hydrocarbons containing 3-9 carbons, adding organotitanium compounds of formulae (I)-(IV) and/or (V), then stirring in the presence of a dry or humid air, removing the solvent and the residue, and after drying, decomposing thermally to air at 200-700 degrees C. An organoaluminum compound in organic solvent is used at a concentration of 0.001-10 mol/l. The concentration of the organotitanium compound in an organic solvent is 0.001-10 mol/l. R1, R1 = 1-9C alkyl; k = 3-4; and n, m = 2.