• 专利标题:   Preparation of graphite thermal field material surface-coated with tantalum carbide coating for high temperature third-generation semiconductor crystal growth furnace, involves high-pressure water treating graphite surface, plasma spraying tantalum powder, infiltrating graphite, and carbonizing.
  • 专利号:   CN113735627-A, CN113735627-B
  • 发明人:   TANG B, WU X
  • 专利权人:   HANGZHOU VULCAN NEW MATERIAL TECHNOLOGY, ZHUJI WOKEN ZHONGZHI NEW MATERIALS CO
  • 国际专利分类:   C04B041/87, C23C004/06, C23C004/134, C30B015/00, C30B035/00
  • 专利详细信息:   CN113735627-A 03 Dec 2021 C04B-041/87 202225 Chinese
  • 申请详细信息:   CN113735627-A CN11036456 06 Sep 2021
  • 优先权号:   CN11036456

▎ 摘  要

NOVELTY - A preparation method of graphite thermal field material surface-coated with tantalum carbide coating, involves (1) surface-processing a surface of a graphite element using high-pressure water containing spherical carbon black, so that the surface of the graphite element becomes uneven, (2) spraying deionized water solution of high-purity tantalum powder and high-purity graphene aqueous solution through a high pressure squirt gun into a container for blending, mixing and filtering, and drying to obtain plasma sprayed powder, (3) plasma spraying the plasma sprayed powder using a laser plasma spraying device, reciprocatingly fast spraying on the surface of the graphite element after surface treatment in the step (1), and (4) infiltrating the graphite element after spraying in the step (3) at 1500-2800degreesC under argon gas atmosphere with tantalum powder, graphene powder and graphite substrate, carbonizing to generate tantalum carbide, and forming tantalum carbide coating. USE - Preparation method of graphite thermal field material surface-coated with tantalum carbide coating (claimed), for use in high temperature third-generation semiconductor crystal growth furnace. ADVANTAGE - The preparation method has high production efficiency, low energy consumption, and low pollution, and provides product with high purity and excellent thermal shock resistance. The formed tantalum carbide coating is dense, high in strength, high in purity and resistant to high temperature erosion. The final drawing strength of the tantalum carbide coating reaches 5 MPa, and the impurity content is controlled below 2 ppm. The graphite thermal field material coated with the tantalum carbide coating on the surface can be directly used in a high-temperature furnace protected by vacuum and inert gas, and can be used stably at a temperature of 1000-2500degreesC.