• 专利标题:   Hierarchical structure carbon-nickel cobalt sulfide-graphene supercapacitor electrode active material is prepared by stirring sodium alginate-chitosan-graphene composite hydrogel, nickel nitrate and cobalt nitrate, reacting and calcining.
  • 专利号:   CN111627721-A
  • 发明人:   LIU D
  • 专利权人:   LIU D
  • 国际专利分类:   H01G011/26, H01G011/32, H01G011/34, H01G011/86
  • 专利详细信息:   CN111627721-A 04 Sep 2020 H01G-011/26 202077 Pages: 11 Chinese
  • 申请详细信息:   CN111627721-A CN10612175 29 Jun 2020
  • 优先权号:   CN10612175

▎ 摘  要

NOVELTY - A hierarchical structure porous carbon-nickel cobalt sulfide-graphene supercapacitor electrode active material is prepared by adding graphene oxide to distilled water, ultrasonically dispersing, reacting at 180-200 degrees C for 6-12 hours, filtering, drying to obtain graphene hydrogel, adding graphene hydrogel, polyvinyl alcohol, sodium alginate and chitosan to distilled water, ultrasonically dispersing, stirring for 5-10 hours, filtering, dialyzing, freeze-drying at -20 degrees C to -5 degrees C for 10-20 hours to obtain sodium alginate-chitosan-graphene composite hydrogel, adding sodium alginate-chitosan-graphene composite hydrogel to distilled water, adding nickel nitrate and cobalt nitrate, ultrasonically dispersing, stirring for 12-24 hours, vacuum drying, adding glycol, citric acid and thioacetamide, stirring, performing microwave treatment, filtering, washing and drying to obtain petal-like nickel cobalt sulfide loaded composite hydrogel and calcining in atmosphere furnace. USE - Hierarchical structure porous carbon-nickel cobalt sulfide-graphene supercapacitor electrode active material. ADVANTAGE - The supercapacitor electrode active material has three-dimensional conductive network which accelerates the transmission and diffusion of electrons and promotes the reversible progress of the pseudo-capacitance redox reaction, so that the hierarchical porous supercapacitor electrode active material exhibits excellent specific capacitance.